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反應特點

反應機理

反應實例

【J. Chem. Soc., Perkin Trans. 1, 1990, 47-65】

【Chem. Lett., 1992, 167-170】

【J. Org. Chem., 2000, 65, 985-989】

【J. Org. Chem., 2000, 65, 5072-5074】

To a 1-dram vial equipped with a magnetic stir bar was added ester (29.2mg, 0.100 mmol, 1.0 equiv), allyl bromide (24.2 mg, 0.200 mmol, 2.0 equiv) and THF (1 mL). DBU (30.4 mg, 0.200 mmol, 2.0 equiv) was added and the reaction was stirred at room temperature for 2 h and then diluted with water and ethyl acetate. The organic was washed with water followed by brine, dried over sodium sulfate and concentrated in vacuo. Flash chromatography provided product (31.2 mg, 0.940 mmol,94% yield) as a white solid.

【J. Am. Chem. Soc., 2012, 134 , 7329–7332】

編譯自：Strategic Applications of Named Reactions in OrganicSnthesis, László Kürti and Barbara Czakó, malonic ester synthesis，page 272-273.

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